1 0 0 20 40 60 timeminutes 80 100 120

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Unformatted text preview: nconditionsresultsinthereaction lackingalltheneededmaterialstoremainfullyreversible;therefore,weplannedtomonitorthe reaction,extractingsmallaliquotsfromthereactionmixtureatthetestingtimesforindividualwork ­up andtesting.Furthermore,duetotimeconstraints,itwasdeterminedthatthereactionwastoberun usingcumeneasthesolvent,ratherthantoluene,duetothefactthatcumenehasahigherboilingpoint andthuswouldallowthereactiontoachievethermodynamiccontrolfasterunderstandardatmospheric refluxthanwithtoluene. 4  Results  FortheNaBH4experiment,weobtainedafinalIsoborneol:Borneolproductratioof5.5:1±0.3, takingintoaccountthe98%purityoftheisoborneol,andthe95%purityoftheborneol.1  FortheAl(OPri)3experiment,resultsofthetestsconductedwerecollectedamongstthevarious groupsperformingtheexperiment,andtheresultingdatawerecompliedinTable5,foundintheSI section.Thefinalproductratioappearstosettleatafinalvalueof2.33593,withastandarddeviationof 0.070739. MPVReductionofCamphor Borneol:IsoborneolRatio 3 2.5 2 Legend: NMJ 1.5 CCEB 1 CMWP 0.5 0 0 20 40 60 80 100 120 Time(minutes)  Figure3:Borneol ­IsoborneolRatiosvs.Time...
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This document was uploaded on 03/27/2014 for the course BIO 403 at Rochester.

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