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Unformatted text preview: edtotheflasktoquenchtheleftoverreactants.Thecontentsoftheflaskwerethen extractedwithdiethyletherandsaturatedsodiumchloridesolution,andtheorganiclayerwas thentestedbyGCfortheproductratios. Meerwein ­Ponndorf ­VerleyReductionofCamphor Al(OPri)3(9.370g,40mmol)was dissolvedincumene(40mL)inaroundbottomflaskplacedinasandbathwithboilingchips.The 7  reactionmixturerefluxedwithawater ­cooledcondenserbeforecamphor(0.610g,4mmol) dissolvedinminimalcumenewasaddedthroughthecondenserintothemixture.Oncethe camphorwasadded,thereactionhadaliquotsextractedviaalongpipettethroughthe condenserevery5minutesforthefirst20minutes,every10minutesforthenext40minutes afterthat,andfinallyevery15minutesf...
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This document was uploaded on 03/27/2014 for the course BIO 403 at Rochester.

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