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3.(5) Create a procedure and dilution for a 325 mg/tablet ASA to be placed in a 1L volumetric flask and diluted to 10.00 ppm in a 10.00 mL volumetric using a micropipette.1
Table 1. Calibration Data.ConcentrationCox and CortezFitz and ClappPatel and DavisWoodyard and HuaBlank0.0008-0.0003-0.0010-0.00014 ppm0.13890.16220.13820.17696 ppm0.21820.28200.22950.25498 ppm0.28380.38710.32090.358810 ppm0.34870.41750.37910.403615 ppm0.54300.51140.54330.644220 ppm0.70740.68490.72980.8639100 ppm 2.83501.64032.78482.8616Unknown 0.37380.23990.35480.3967Unknown + 10 ppm Spike0.73230.58770.71570.5058ConcentrationMalone and HarryWasdin and GreeneArroyave and NguyenOja and MillerBlank0.00060.00180.0000-0.00024 ppm0.14430.13620.13820.17006 ppm0.22210.20630.21370.24328 ppm0.28710.32010.29560.314210 ppm0.36620.40210.35520.458315 ppm0.54370.60780.54280.581320 ppm0.72040.78310.72250.7375100 ppm 2.77892.69052.68902.7551Unknown 0.43880.28950.16260.3798Unknown + 10 ppm Spike0.89480.67550.52510.3083ConcentrationPearson and WatsonAverage Standard DeviationBlank-0.00030.00010.000814 ppm0.21830.15810.027316 ppm0.28390.23930.028848 ppm0.29270.31780.0348810 ppm0.37470.39250.0370715 ppm0.55390.56350.0406920 ppm0.77100.74670.05322100 ppm 1.97162.55630.43714Unknown 0.58860.35830.12184Unknown + 10 ppm Spike0.76370.63430.17299Results and Discussion – 10 points each. 1.Examine the pooled class data and reject outliers using the Grubb’s test.The rejected outliers would be 0.2183 and 0.86392.Provide an external calibration curve of the linear range, with cleaned up formatting and appropriate error bars. To add error bars, click on your graph and pick Chart Tools – Designon the Excel tool bar (top right). Go to Add Chart Elements drop down menu and select error bars and more error bars options. Choose vertical error bars, both directions and the error amount to be a custom range. Put in the cells that