E 4 Na acut e Skin irritati on toluene 921 4 087 mL 46 E 4 na Acut e

# E 4 na acut e skin irritati on toluene 921 4 087 ml

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E-4 Na acut e Skin irritati on toluene 92.1 4 0.87 110 -93 ~ 10 mL 4.6 E-4 na Acut e flamm able Calculations: 1. Calculate the number of moles of 1-bromododecane, and N,N,N’,N’- tetramethylethylenediamine used in part I. What is the limiting reagent? 1.4E-4 moles 1-b x 1 / 2 = 7.0 E-5 2.9E-5 moles N x 1/ 1 = 2.9E-5 2. Calculate the theoretical yield of 12-2-12. [Note that you should include the two bromides (Br - ) in your calculation of the molecular mass.] 7.0E-5 x 1015.4/1 = 7.1E-2 Flow chart Part I: A. Combine 1.0 mL acetone, 3.1 mL 1-bromododecane ), and 0.65 mL N,N,N’,N’- tetramethylethylenediamine in 25 mL Erlenmeyer flask mix reagents let flask sit 1 week at room temp add acetone after week is up use vacuum filtration to separate solid weigh, determine MP and calculate % yield of solid B. Get magnetic stir plate attach heating mantle to variac Combine 1.0 mL acetone, 3.1 mL 1-bromododecane ), and 0.65 mL N,N,N’,N’-tetramethylethylenediamine in 25 mL round bottom flask heat rxn for 60 min at 15-20 mL acetone after cooling cool in ice bath vacuum filtrate solid

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• Fall '19
• Solvent, Trigraph, Erlenmeyer flask, ml N

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